Characteristics Analysis of Different Glutinous Rice Flour and Its Influence on Freezing Point Temperature
-
摘要: 为明确不同糯米的粉质特性对冰点温度的影响,以实际应用中具有代表性的25种糯米粉为试验材料,测定其理化特性,通过相关性分析和主成分分析,探讨糯米粉原料特性对冰点温度的影响。结果表明,25种糯米粉粉团的冰点温度分布在−1.35~−2.65 ℃之间;脂肪含量与冰点温度成显著负相关(P<0.05),而蛋白质、淀粉、灰分与冰点温度之间不存在明显的依存关系;糯米粉热特性、吸水率、溶解度、胶稠度和平均粒径与冰点温度均呈极显著负相关(P<0.01)。主成分分析结果显示,影响糯米粉冰点温度的关键特性为糯米粉的平均粒径、热特性(峰值温度、起始温度、终止温度)、最终粘度、粗脂肪含量和溶解度。研究结果可为冰点冷冻汤圆工业化生产时合理选择糯米粉提供理论依据,实验范围内,优糯6211、黑糯米纯粉、预糊化糯米粉较为适合制作冰点冷冻汤圆。Abstract: In order to the main influence factors of glutinous rice farinographical properties on freezing point temperature, 25 representative glutinous rice flours in practical applications were used as test materials, and the physical and chemical properties of the glutinous rice flours were measured. Through correlation analysis and principal component analysis, the influence of the raw material characteristics of glutinous rice flour on the freezing point temperature was discussed. The results showed that the freezing point temperature of the 25 kinds of glutinous rice flour was between −1.35~−2.65 ℃. The fat content had a significant negative correlation with the freezing point temperature (P<0.05), while there was no obvious dependence between protein, starch, ash and freezing point temperature. The thermal properties, water absorption, solubility, gel consistency and average particle size of glutinous rice flour were all significantly negatively correlated with the freezing point temperature (P<0.01). Principal component analysis results showed that the key factors affecting the freezing point temperature of glutinous rice flour were mainly the average particle size of glutinous rice flour, the thermal characteristics of glutinous rice flour (peak temperature, starting temperature, ending temperature), final viscosity, crude fat content and solubility. The research results could provide a theoretical basis for the rational selection of raw materials for the industrial production of glutinous rice flour with freezing point frozen glutinous rice balls. Within the scope of the experiment, Younuo 6211, pure black glutinous rice flour, and pre-gelatinized glutinous rice flour are more suitable for making freezing point frozen tangyuan.
-
Key words:
- glutinous rice flour /
- composition /
- physical and chemical index /
- freezing point
-
表 1 不同糯米粉基本成分分析
Table 1. Analysis of the basic components of different glutinous rice flour
样品 水分(%) 灰分(%) 淀粉(%) 破损淀粉(%) 蛋白质(%) 脂肪(%) 糯优2号 11.2±0.11h 0.23±0.01m 86.49±0.37i 3.52±0.01u 5.89±0.08o 0.71±0.01lm 优糯6211 9.70±0.15l 0.16±0.00o 90.40±0.11cd 4.24±0.03p 5.62±0.06p 0.61±0.03n 绍糯9714 10.50±0.14j 0.21±0.01n 86.30±0.45i 3.82±0.05t 8.44±0.04c 1.22±0.01g 血糯 10.10±0.13k 0.23±0.01m 90.85±0.11bc 5.22±0.01m 6.54±0.06lm 2.65±0.05b 嘉糯1优6号 10.30±0.15jk 0.33±0.01i 91.13±0.13ab 5.62±0.01j 8.23±0.05d 1.05±0.04h 皖垦糯 8.60±0.20n 0.23±0.00m 88.29±0.11g 5.76±0.04g 9.15±0.06a 0.84±0.01k 武育糯16号 11.50±0.42efg 0.17±0.01o 85.15±0.17jk 6.20±0.01c 8.73±0.06b 0.76±0.02l 苏御糯 11.30±0.10gh 0.53±0.01e 83.46±0.41m 6.06±0.03e 7.48±0.04g 0.68±0.01m 丹旱稻53 10.30±0.21jk 0.17±0.01o 91.49±0.31a 4.91±0.04n 9.15±0.08a 0.73±0.06lm 连糯1号 9.50±0.09l 0.26±0.01l 86.59±0.21i 3.84±0.08t 7.24±0.06hi 0.60±0.01n 南粳46 9.20±0.08m 0.38±0.01g 90.12±0.37de 5.36±0.04l 5.38±0.06q 0.82±0.05k 东北粳糯 11.60±0.01ef 0.43±0.01f 91.65±0.20a 4.94±0.01n 6.20±0.03n 0.84±0.01k 江西籼糯 11.20±0.02h 0.23±0.01m 88.88±0.19f 5.74±0.02gh 6.44±0.03m 0.98±0.02i 安徽粳糯 10.50±0.01j 0.31±0.01j 86.62±0.66i 5.65±0.03ij 6.57±0.08l 1.76±0.03d 信阳籼糯 10.90±0.01i 0.56±0.01d 87.40±0.17h 6.10±0.03de 6.74±0.11k 0.84±0.02k 浙江籼糯 11.40±0.01fgh 0.36±0.00h 83.31±0.31n 5.85±0.05f 7.74±0.02e 0.59±0.04n 2014越南籼糯 12.40±0.02b 0.26±0.01l 84.77±0.31kl 4.53±0.02o 7.61±0.04f 0.76±0.01l 吉林粳糯 12.10±0.03c 0.28±0.01k 91.49±0.13a 5.46±0.01k 7.01±0.10j 1.27±0.08g 湖南水磨籼糯米粉 11.90±0.01cd 0.29±0.01k 88.40±0.07fg 6.34±0.01b 7.17±0.06i 0.74±0.03lm 泰国水磨糯米粉 12.60±0.01b 0.28±0.01k 85.47±0.10j 6.51±0.02a 7.32±0.09h 1.54±0.06e 河北粳糯水磨粉 12.90±0.02a 0.58±0.01c 91.24±0.60ab 6.13±0.03d 5.99±0.13o 1.33±0.01f 半干法黑糯米纯粉 11.70±0.03de 1.14±0.01b 89.54±0.54e 4.04±0.01r 8.67±0.06b 2.07±0.03c 黑糯米纯粉 10.30±0.05jk 1.22±0.02a 89.76±0.11e 4.10±0.01q 8.22±0.04d 3.18±0.05a 半干法辊磨粳糯米 11.60±0.08ef 0.34±0.01i 89.94±0.38de 5.69±0.04hi 8.27±0.05d 0.92±0.01j 预糊化糯米粉 7.80±0.08o 0.22±0.01mn 84.56±0.28lm 3.92±0.01s 5.65±0.10p 1.72±0.02d 注:表中基本成分(除水分)的数据均为干基;同列不同小写字母表示差异显著(P<0.05),表2~表4同。 表 2 糯米粉的理化性质
Table 2. The physicochemical properties of glutinous rice flour
样品 (D90-D10)/D50 Dav(μm) 吸水率(%) 溶解度(%) 胶稠度(mm) 膨胀能力(mL·g−1) 糯优2号 1.58±0.01c 6.87±0.57q 2.24±0.01efghij 0.77±0.03i 142.20±0.48i 4.30±0.21t 优糯6211 1.46±0.01f 7.47±0.04p 2.15±0.03ghijk 1.25±0.02e 162.20±0.27c 3.90±0.19t 绍糯9714 1.57±0.02c 8.56±0.02mn 2.15±0.01ghijk 1.15±0.01f 109.00±0.11p 7.70±0.17r 血糯 1.69±0.03b 6.59±0.06q 2.26±0.02efghi 0.51±0.04m 129.40±0.61l 35.70±0.21a 嘉糯1优6号 1.43±0.01f 8.26±0.03n 2.21±0.02fghij 0.68±0.01j 155.50±0.33e 17.30±0.46m 皖垦糯 1.43±0.01f 7.77±0.01op 2.08±0.01jkl 0.55±0.00kl 116.40±0.20n 32.70±0.29d 武育糯16号 1.57±0.05c 7.92±0.11o 2.14±0.02hijk 0.27±0.02p 155.40±0.52e 34.00±0.18c 苏御糯 1.66±0.11b 9.60±0.12l 1.95±0.01l 0.38±0.01no 85.00±0.49r 12.30±0.50o 丹旱稻53 1.45±0.02f 8.86±0.03m 2.09±0.01ijkl 0.41±0.00n 115.10±0.60o 4.90±0.050s 连糯1号 1.52±0.03de 7.79±0.07op 2.22±0.02efghij 0.25±0.02p 146.00±0.45g 35.20±0.30b 南粳46 1.50±0.00e 8.26±0.03n 2.00±0.01kl 0.41±0.01n 72.90±0.50s 11.70±0.20p 东北粳糯 1.70±0.01b 6.62±0.02q 2.34±0.01def 0.87±0.02h 108.60±0.38p 9.90±0.18q 江西籼糯 1.28±0.01g 7.54±0.01p 2.07±0.01jkl 0.52±0.04lm 119.30±0.11m 19.90±0.06j 安徽粳糯 1.82±0.02a 10.53±0.19k 2.15±0.02ghijk 0.56±0.01k 132.70±0.16k 35.50±0.04ab 信阳籼糯 1.55±0.05cd 8.44±0.27n 2.27±0.00efgh 0.85±0.02h 143.80±0.06h 20.40±0.22i 浙江籼糯 1.29±0.06g 60.47±0.14c 2.44±0.01d 1.07±0.01g 155.60±0.29e 25.10±0.47g 2014越南籼糯 0.80±0.01k 45.79±0.06f 2.35±0.00def 1.65±0.00c 154.90±0.24e 27.70±0.04f 吉林粳糯 1.12±0.02h 55.46±0.42e 2.16±0.01ghijk 0.37±0.02o 142.80±0.26i 13.90±0.02n 湖南水磨籼糯米粉 0.86±0.00j 39.13±0.02g 2.22±0.04efghij 0.40±0.01no 162.10±0.30c 19.10±0.17k 泰国水磨糯米粉 0.92±0.02i 38.61±0.04h 2.38±0.01de 0.67±0.01j 151.40±0.45f 28.40±0.31e 河北粳糯水磨粉 1.15±0.01h 57.67±0.22d 2.32±0.01defg 0.53±0.04klm 170.00±0.78a 25.50±0.21g 半干法黑糯米纯粉 1.12±0.00h 21.61±0.03j 3.01±0.04b 1.67±0.03c 134.30±0.16j 7.80±0.11r 黑糯米纯粉 1.42±0.02f 23.53±0.20i 2.43±0.03d 2.17±0.01b 160.00±0.62d 9.70±0.15q 半干法辊磨粳糯米 0.89±0.01ij 78.11±0.28b 2.60±0.01c 1.53±0.01d 89.40±0.45q 18.30±0.45l 预糊化糯米粉 1.30±0.01g 88.05±0.22a 6.86±0.43a 2.26±0.02a 165.20±0.45b 21.50±0.11h 表 3 糯米粉糊化特性分析
Table 3. The pasting characteristics of the glutinous rice flour
样品 峰值粘度(mP·s) 谷值粘度(mP·s) 衰减值(mP·s) 最终粘度(mP·s) 回生值(mP·s) 糊化温度(℃) 糯优2号 1242.00±2.80h 572.00±1.40p 670.00±1.40hijk 741.00±5.70o 169.00±4.20k 80.40±0.60b 优糯6211 1449.00±9.90gh 768.00±0.00m 681.00±9.90hijk 952.00±4.20l 184.00±4.20j 83.23±0.10b 绍糯9714 616.00±7.10i 205.50±3.50r 410.50±3.50jk 297.00±4.20q 91.50±0.70m 71.88±0.00cde 血糯 1657.50±6.40efg 666.00±0.00o 991.50±6.40efghi 836.00±2.80n 170.00±2.80k 69.83±0.60def 嘉糯1优6号 1255.00±18.40h 570.50±14.80p 684.50±3.50hijk 756.50±19.10o 186.00±4.20j 80.40±0.60b 皖垦糯 1887.00±1.40def 965.00±7.10ij 922.00±5.70fghi 1270.50±4.90h 305.50±2.10d 72.68±0.00cde 武育糯16号 2198.50±6.40d 1016.50±0.70gh 1182.00±7.10defg 1250.50±3.50h 234.00±4.20gh 69.85±0.60def 苏御糯 2143.00±25.50d 1335.00±1.40e 808.00±240ghij 1798.50±3.50e 463.50±2.10b 72.60±0.00cde 丹旱稻53 576.50±4.90i 263.50±0.70q 313.00±5.70k 366.50±2.10p 103.00±1.40l 73.10±0.60cd 连糯1号 1844.00±19.80defg 856.00±4.20l 988.00±24.00efghi 1092.00±4.20k 236.00±0.00gh 70.25±0.00def 南粳46 1573.50±0.70fgh 855.00±33.90l 718.50±33.20hijk 1243.00±32.50h 388.00±1.40c 73.50±1.30cd 东北粳糯 2238.00±1.40d 948.50±0.70jk 1289.50±2.10def 1133.50±7.80j 185.00±7.10j 68.25±0.50ef 江西籼糯 1719.00±9.90efg 1000.00±0.00h 719.00±9.90hijk 1256.00±9.90h 256.00±9.90f 73.55±0.00cd 安徽粳糯 1713.00±5.70efg 715.00±7.10n 998.00±12.70efghi 912.50±2.10m 197.50±4.90i 69.90±0.70def 信阳籼糯 1693.50±26.20efg 1108.00±15.60f 585.50±10.60ijk 1346.50±7.80g 238.50±7.80gh 81.18±0.50b 浙江籼糯 3458.00±8.50b 1651.00±4.20c 1807.00±4.20b 1880.50±3.50d 229.50±0.70h 69.45±0.10def 2014越南籼糯 3233.00±0.00b 1811.00±5.70b 1422.00±5.70cd 2083.50±7.80c 272.50±2.10e 70.63±0.50def 吉林粳糯 1649.50±4.90efg 922.00±7.10k 727.50±12.00hijk 1127.00±12.70j 205.00±5.70i 72.28±0.70cde 湖南水磨籼糯米粉 2215.50±19.10d 986.00±2.80hi 1229.50±16.30def 1242.50±4.90h 256.50±7.80f 71.85±1.10cde 泰国水磨糯米粉 4019.00±28.30a 2302.50±2.10a 1716.50±26.20bc 2606.50±9.20a 304.00±7.10d 70.18±0.00def 河北粳糯水磨粉 2723.50±6.40c 1369.00±0.00d 1354.50±6.40cde 1612.50±3.50f 243.50±3.50g 66.075±0.00f 半干法黑糯米纯粉 1624.00±15.60efgh 1037.00±56.60g 587.00±41.00ijk 2213.00±55.20b 1176.00±1.40a 91.70±0.60a 黑糯米纯粉 573.00±7.10i 175.00±2.80s 398.00±4.20jk 251.50±3.50r 76.50±0.70n 71.025±0.00de 半干法辊磨粳糯米 2001.50±9.20de 933.50±6.40k 1068.00±2.80defgh 1208.50±3.50i 275.00±9.90e 68.10±0.60ef 预糊化糯米粉 3096.50±862.00b 565.00±5.70p 2531.50±867.60a 848.00±7.10n 283.00±1.40e 75.75±9.20c 表 4 糯米粉的冰点与热特性测定
Table 4. The freezing point and thermal properties of glutinous rice flour
样品 冰点温度(℃) 起始温度(℃) 峰值温度(℃) 终止温度(℃) 糊化焓ΔH(J·g−1) 糯优2号 −2.10±0.00hij 74.40±0.28a 78.15±0.07c 83.75±0.21c 3.35±0.00a 优糯6211 −2.55±0.07l 74.60±0.14a 78.55±0.35c 82.65±0.64d 3.12±0.07b 绍糯9714 −1.75±0.07ef 60.25±0.07fg 68.45±0.07fg 73.65±0.21kl 1.94±0.07j 血糯 −1.85±0.07fg 65.00±0.28cd 66.75±0.35hi 72.80±0.28lmn 1.69±0.00l 嘉糯1优6号 −2.05±0.07hij 74.05±0.49a 78.35±0.64c 81.45±0.64e 1.52±0.02m 皖垦糯 −2.30±0.00k 64.90±0.42d 70.56±0.08de 75.90±0.85fgh 2.07±0.08i 武育糯16号 −2.20±0.14jk 63.30±0.57e 68.35±0.64fg 72.75±0.49lmn 1.81±0.02k 苏御糯 −1.50±0.14bc 59.90±0.14fg 65.95±0.64i 72.65±0.35mn 1.72±0.00l 丹旱稻53 −1.35±0.07a 64.60±0.85d 70.35±0.64de 75.25±0.35hi 2.63±0.01c 连糯1号 −1.97±0.06gh 62.80±0.42e 68.20±0.99fg 73.30±0.57klm 2.41±0.02e 南粳46 −1.68±0.05de 60.75±0.35f 67.35±0.21gh 72.55±0.64mn 2.21±0.10gh 东北粳糯 −1.40±0.14ab 59.60±0.57g 66.90±0.42hi 72.45±0.49mn 2.14±0.02hi 江西籼糯 −2.05±0.07hij 65.70±0.42c 71.30±0.28d 76.25±0.07fg 1.53±0.07m 安徽粳糯 −1.55±0.07cd 59.45±0.78g 65.75±0.78ij 72.80±0.28lmn 2.32±0.08f 信阳籼糯 −2.10±0.14hij 74.55±0.64a 80.00±0.99b 84.95±0.49b 2.37±0.05ef 浙江籼糯 −1.60±0.14cde 59.80±0.85fg 66.90±0.28hi 72.00±0.85n 2.50±0.09d 2014越南籼糯 −2.00±0.00ghi 62.40±0.28e 68.70±0.28f 74.60±0.28ij 2.24±0.03g 吉林粳糯 −2.05±0.07hij 62.65±0.21e 70.40±0.28de 76.45±0.35f 2.18±0.03gh 湖南水磨籼糯米粉 −2.05±0.07hij 64.50±0.85d 70.15±0.64de 75.35±0.78ghi 2.50±0.01d 泰国水磨糯米粉 −1.65±0.07cde 62.90±1.27e 69.90±0.99e 73.90±0.42jk 0.78±0.00p 河北粳糯水磨粉 −2.15±0.07ijk 54.35±0.78h 64.10±0.85k 69.30±0.57o 1.93±0.06j 半干法黑糯米纯粉 −1.85±0.07fg 60.50±0.42fg 64.70±1.70jk 68.95±0.21o 0.98±0.01o 黑糯米纯粉 −2.55±0.07l 62.40±0.42e 68.65±0.64f 75.55±0.49fgh 1.41±0.02n 半干法辊磨粳糯米 −2.15±0.07ijk 72.35±0.64b 81.25±0.21a 86.10±0.85a 1.35±0.02n 预糊化糯米粉 −2.65±0.07l 72.65±0.78b 77.80±0.85c 84.30±0.57bc 1.96±0.02j 表 5 糯米粉冰点温度与理化性质的相关性分析
Table 5. Correlation analysis between the freezing point and physicochemical properties of glutinous rice flour
指标 冰点温度 指标 冰点温度 蛋白质 0.12 膨胀能力 0.01 灰分 −0.11 胶稠度 −0.44** 脂肪 −0.30* 峰值粘度 0.05 淀粉 0.09 谷值粘度 0.22 峰值温度 −0.50** 衰减值 −0.12 起始温度 −0.52** 最终粘度 0.21 终止温度 −0.51** 回生值 0.08 糊化焓 −0.01 糊化温度 −0.25 吸水率 −0.41** Dav −0.31** 溶解度 −0.50** 注:**表示在0.01水平上极显著相关;*表示在0.05水平上显著相关。 表 6 影响糯米粉冰点温度的指标主成分分析
Table 6. Principal component analysis of indicators that affect the freezing point of glutinous rice flour
项目 1 2 3 4 5 6 特征根 6.54 5.04 3.28 2.07 1.52 1.23 贡献率(%) 27.23 21.01 13.66 8.63 6.34 5.12 累计贡献率(%) 27.23 48.24 61.90 70.53 76.87 81.99 表 7 影响冰点温度的指标正交旋转因子载荷
Table 7. The orthogonal rotation factor load of the index that affects the freezing temperature
1 2 3 4 5 6 共同度 Dav(μm) 0.98 0.05 0.09 0.06 0.08 0.01 0.98 粗蛋白(%) −0.06 0.00 −0.02 −0.02 0.03 0.84 0.72 粗灰分(%) −0.00 −0.28 0.20 −0.43 0.66 0.21 0.79 粗脂肪(%) 0.06 −0.23 −0.24 0.01 0.84 0.20 0.86 粗淀粉(%) −0.22 0.00 0.00 −0.09 0.00 −0.06 0.81 吸水率(%) 0.54 0.31 −0.04 0.17 0.50 −0.31 0.84 溶解度(%) 0.48 0.25 −0.02 −0.23 0.63 −0.01 0.73 膨胀能力(mL·g−1) 0.04 −0.15 0.08 0.89 −0.02 0.21 0.87 胶稠度(mm) 0.21 0.22 0.05 0.38 0.41 −0.14 0.59 峰值粘度(mP·s) 0.53 −0.09 0.59 0.54 −0.09 −0.14 0.96 谷值粘度(mP·s) 0.28 −0.18 0.80 0.33 −0.24 0.06 0.95 衰减值(mP·s) 0.63 0.01 0.25 0.60 0.09 −0.29 0.90 最终粘度(mP·s) 0.21 −0.20 0.93 0.18 −0.08 0.08 0.99 回生值(mP·s) −0.07 −0.12 0.72 −0.27 0.35 0.08 0.91 糊化温度(℃) −0.35 0.51 0.39 −0.41 0.39 −0.16 0.91 峰值温度(℃) 0.15 0.95 −0.12 −0.12 −0.11 −0.01 0.96 起始温度(℃) −0.03 0.97 −0.10 −0.07 0.00 −0.06 0.97 终止温度(℃) 0.20 0.92 −0.20 −0.12 −0.08 −0.06 0.94 糊化焓ΔH(J·g−1) −0.15 0.21 −0.28 −0.07 −0.42 −0.63 0.73 -
[1] LI Y, DING G, YOKOYAMA W, et al. Characteristics of annealed glutinous rice flour and its formation of fast-frozen dumplings[J]. Journal of Cereal Science,2018,79:106−112. doi: 10.1016/j.jcs.2017.09.016 [2] 夏露, 张超, 王立, 等. 冬小麦抗冻蛋白制备及其在汤圆中的应用研究[J]. 食品工业科技,2009,30(11):241−243, 310. [XIA L, ZHANG C, WANG L, et al. Preparation and application of antifreeze proteins extracted from winter wheat bran[J]. Science and Technology of Food Industry,2009,30(11):241−243, 310.XIA L, ZHANG C, WANG L, et al. Preparation and application of antifreeze proteins extracted from winter wheat bran[J]. Science and Technology of Food Industry, 2009, 30(11): 241-243, 310. [3] 张国治. 糯米粉的品质分析及速冻汤圆品质改良[J]. 冷饮与速冻食品工业,2006,12(2):39−42. [ZHANG G Z. Property analysis of flour of glutinous rice and quality of deep-frozen glutinous rice dough[J]. Beverage & Fast Frozen Food Industry,2006,12(2):39−42.ZHANG G Z. Property analysis of flour of glutinous rice and quality of deep-frozen glutinous rice dough[J]. Beverage & Fast Frozen Food Industry, 2006, 12(2): 39-42. [4] 周显青, 胡育铭, 张玉荣, 等. 我国速冻汤圆加工及其质量控制技术现状与展望[J]. 粮油食品科技,2014,22(2):6−11. [ZHOU X Q, HU Y M, ZHANG Y R, et al. Status and prospects of processing and quality control for the frozen rice dumplings in China[J]. Science and Technology of Cereals, Oils and Foods,2014,22(2):6−11. doi: 10.3969/j.issn.1007-7561.2014.02.002ZHOU X Q, HU Y M, ZHANG Y R, et al. Status and prospects of processing and quality control for the frozen rice dumplings in China[J]. Science and Technology of Cereals, Oils and Foods, 2014, 22(2): 6-11. doi: 10.3969/j.issn.1007-7561.2014.02.002 [5] 李真, 安阳, 艾志录, 等. 基于响应面法优化工艺参数改善速冻汤圆品质[J]. 食品与发酵工业,2017,43(8):163−168. [LI Z, AN Y, AI Z L, et al. Optimization of quick-frozen Tang-yuan processing by response surface method[J]. Food and Fermentation Industries,2017,43(8):163−168.LI Z, AN Y, AI Z L, et al. Optimization of quick-frozen Tang-yuan processing by response surface method[J]. Food and Fermentation Industries, 2017, 43(8): 163-168. [6] CAI J W, CHIANG J H, TAN M, et al. Physicochemical properties of hydrothermally treated glutinous rice flour and xanthan gum mixture and its application in gluten-free noodles[J]. Journal of Food Engineering,2016,186(10):1−9. [7] LI Z N, WANG L, CHEN Z X, et al. Impact of protein content on processing and texture properties of waxy rice flour and glutinous dumpling[J]. Journal of Cereal Science,2018(81):30−36. [8] 陈瑾. 速冻汤圆品质与糯米粉粉质相关性及糯米粉配粉研究[D]. 郑州: 河南农业大学, 2019CHEN J. Study on the correlation between the quality of quick-frozen dumplings and the quality of gulutinous rice flour and the powdering of glutinous rice flour[D]. Zhengzhou: Henan Agricultural University, 2019. [9] 黄忠民, 陈瑾, 宋会玲, 等. 糯米粉特性与速冻汤圆品质相关性分析[J]. 食品工业科技,2019,40(4):93−99. [HUANG Z M, CHEN J, SONG H L, et al. Correlation between the characteristics of glutinous rice flour and quality[J]. Science and Technology of Food Industry,2019,40(4):93−99.HUANG Z M, CHEN J, SONG H L, et al. Correlation between the characteristics of glutinous rice flour and quality[J]. Science and Technology of Food Industry, 2019, 40(4): 93-99. [10] 孙威, 陈轩, 庄坤, 等. 调质温度和时间对黑糯米半干法制粉品质的影响[J]. 食品工业科技,2020,41(5):17−22, 30. [SUN W, CHEN X, ZHUANG K, et al. Effect of tempering temperature and time on the quality of semi-dry black glutinous rice flour[J]. Science and Technology of Food Industry,2020,41(5):17−22, 30.SUN W, CHEN X, , ZHUANG K, et al. Effect of tempering temperature and time on the quality of semi-dry black glutinous rice flour[J]. Science and Technology of Food Industry, 2020, 41(5): 17-2, 30. [11] CJAM K, TVANV, WALSTRA P. Gelation and retrogradation of concentrated starch systems: 2. Retrogradation[J]. Food Hydrocolloids,1996,10(3):355−362. doi: 10.1016/S0268-005X(96)80012-9 [12] 付一帆, 甘淑珍, 赵思明. 几种淀粉的糊化特性及力学稳定性[J]. 农业工程学报,2008,24(10):255−257. [FU Y F, GAN S Z, ZHAO S M. Gelatinization characteristics and mechanical stability of various starch sources[J]. Transactions of the CSAE,2008,24(10):255−257. doi: 10.3321/j.issn:1002-6819.2008.10.052FU Y F, GAN S Z, ZHAO S M. Gelatinization characteristics and mechanical stability of various starch sources[J]. Transactions of the CSAE, 2008, 24(10): 255-257. doi: 10.3321/j.issn:1002-6819.2008.10.052 [13] 顾玲, 张燕萍. 杂粮粉对糯米粉理化性质的影响[J]. 食品科技,2015,40(2):186−190. [GU L, ZHANG Y P. Impact of grains powder on the physicochemical properties of glutinous rice flour[J]. Food Science and Technology,2015,40(2):186−190.GU L, ZHANG Y P. Impact of grains powder on the physicochemical properties of glutinous rice flour[J]. Food Science and Technology, 2015, 40(2): 186-190. [14] 钟志友, 张敏, 杨乐, 等. 果蔬冰点与其生理生化指标关系的研究[J]. 食品工业科技,2011,32(2):76−78. [ZHONG Z Y, ZHANG M, YANG L, et al. Study on relation between freezing and physiological and biochemical indexes of fruits and vegetable[J]. Science and Technology of Food Industry,2011,32(2):76−78.ZHONG Z Y, ZHANG M, YANG L, et al. Study on relation between freezing and physiological and biochemical indexes of fruits and vegetable[J]. Science and Technology of Food Industry, 2011, 32(2): 76-78. [15] ISM Z, ABSAR N, KIM S J, et al. Dsc study of mixtures of wheat flour and potato, sweet potato, cassava, and yam starches[J]. Journal of Food Engineering,2008,86(1):68−73. doi: 10.1016/j.jfoodeng.2007.09.011 [16] CHANVRIER H, UTHAYAKUMARAN S, APPELQVIST I A M, et al. Influence of storage conditions on the structure, thermal behavior, and formation of enzyme-resistant starch in extruded starches[J]. Journal of Agricultural & Food Chemistry,2007,55(24):90−98,83. [17] LIN Z, GENG D H, QIN W, et al. Effects of damaged starch on glutinous rice flour properties and sweet dumpling qualities[J]. International Journal of Biological Macromolecules,2021,181:390−397. doi: 10.1016/j.ijbiomac.2021.03.160 [18] 宋莹莹. 糯米粉吸水率影响因素的研究[D]. 武汉: 武汉轻工大学, 2013SONG Y Y. Study on the impacting factors of water absorption of waxy rice flour[D]. Wuhan: Wuhan Polytechnic University, 2013. [19] ZHANG H, WU F, XU D, et al. Effects of milling methods on the properties of glutinous rice flour and sweet dumplings[J]. Journal of Food Science and Technology Mysore,2020,58,(5):1848−1857. [20] ERCOLINI D. Pcr-dgge fingerprinting: Novel strategies for detection of microbes in food[J]. Journal of Microbiological Methods,2004,56(3):297−314. doi: 10.1016/j.mimet.2003.11.006 [21] 田斌强, 邓乾春, 谢笔钧. 发芽燕麦淀粉的热特性[J]. 现代食品科技,2014,30(5):98−103. [TIAN B Q, DENG Q C, XIE B J. Thermal properties of the starch from germinated oat[J]. Modern Food Science and Technology,2014,30(5):98−103.TIAN B Q, DENG Q C, XIE B Y. Thermal properties of the starch from germinated oat[J]. Modern Food Science and Technology, 2014, 30(5): 98-103. [22] KOZLOV I I, SIA S. Effect of amylose content on gelatinization, retrogradation and pasting properties of flours from different cultivars of thai rice[J]. Starch-Stärke,2003,55(9):410−415. [23] PARK I M, IBANEZ A M, ZHONG F, et al. Gelatinization and pasting properties of waxy and non-waxy rice starches[J]. Starch-Stärke,2007,59(8):388−396. [24] 余世锋, 张永春, 林佳楠, 等. 玉米淀粉、绿豆淀粉和皱皮豌豆淀粉热特性及回生性质的比较[J]. 食品科技,2013,38(9):136−140. [YU S F, ZHANG Y C, LIN J N, et al. Comparing the thermal and retrogradation properties of corn starch and mung bean starch and wrinkled pea starch[J]. Food Science and Technology,2013,38(9):136−140.YU S F, ZHANG Y C, LIN J N, et al. Comparing the thermal and retrogradation properties of corn starch and mung bean starch and wrinkled pea starch[J]. Food Science and Technology, 2013, 38(9): 136-140. [25] REDDY C K, CHOI S M, LEE D J, et al. Complex formation between starch and stearic acid: Effect of enzymatic debranching for starch[J]. Food Chemistry,2018,244:136. doi: 10.1016/j.foodchem.2017.10.040 [26] 刘延奇, 秦令祥, 吴史博, 等. 淀粉-脂质复合物的相互作用及研究进展[J]. 食品科技,2009,34(7):209−213. [LIU Y Q, QIN L X, WU S B, et al. Interaction and progress of starch-lipid complex[J]. Food Science and Technology,2009,34(7):209−213.LIU Y Q, QIN L X, WU S B, et al. Interaction and progress of starch-lipid complex[J]. Food Science and Technology, 2009, 34(7): 209-213. [27] 胡烨, 何建东, 王朋, 等. 养殖大黄鱼冰点调节剂研制[J]. 中国食品学报, 2013, 13(1): 51−60HU Y, HE J D, WANG P, et al. Development of freezing-point regulator for cultured large yellow croaker[J]. Journal of Chinese Institute of Food Science and Technology, 2013, 13(1): 51−60. [28] ABBAS T, LAVADIYA D N, KIRAN R. Exploring the use of polyols, corn, and beet juice for decreasing the freezing point of brine solution for deicing of pavements[J]. Sustainability,2021,13(11):5765. doi: 10.3390/su13115765 [29] 李贤勇, 王元凯, 王楚桃. 稻米蒸煮品质与营养品质的相关性分析[J]. 西南农业学报,2001,14(3):21−24. [LI X Y, WANG Y K, WANG C T. Analysis of correlation between quality characters of cooking and nutrition[J]. Southwest China Journal of Agricultural Sciences,2001,14(3):21−24. doi: 10.3969/j.issn.1001-4829.2001.03.005LI X Y, WANG Y K, WANG C T. Analysis of correlation between quality characters of cooking and nutrition[J]. Southwest China Journal of Agricultural Sciences, 2001, 14(3): 21-24. doi: 10.3969/j.issn.1001-4829.2001.03.005 [30] 曹松, 周洲, 董明, 等. 不同实验室干法制备工艺对糯米粉品质特性的影响[J]. 现代食品,2021(17):60−63, 69. [CAO S, ZHOU Z, DONG M, et al. Effects of dry preparation processes in different laboratories on the quality characteristics of glutinous rice flour[J]. Modern Food,2021(17):60−63, 69.CHAO S, ZHOU Z, DONG M, et al. Effects of dry preparation processes in different laboratories on the quality characteristics of glutinous rice flour[J]. Modern Food, 2021(17): 60-63, 69. [31] 余世锋, 杨秀春, MENAGER L, 等. 直链淀粉、蛋白质及脂类对大米粉热特性的影响[J]. 食品与发酵工业,2009,35(4):38−42. [YU S F, YANG X C, MENAGER L, et al. Effects of amylose, protein and lipid on the thermal properties of rice flour[J]. Food and Fermentation Industries,2009,35(4):38−42.YU S F, YANG X C, MENAGER L, et al. Effects of amylose, protein and lipid on the thermal properties of rice flour [J]. Food and Fermentation Industries, 2009, 35(4): 38-42. [32] 应月, 李保国, 董梅, 等. 冰温技术在食品贮藏中的研究进展[J]. 制冷技术,2009,29(2):12−15. [YING Y, LI B G, DONG M, et al. Advances in ice-temperature technique for food storage[J]. Refrigeration Technology,2009,29(2):12−15.YING Y, LI B G, DONG M, et al. Advances in ice-temperature technique for food storage[J]. Refrigeration Technology, 2009, 29(2): 12-15. [33] 赵凯, 张守文, 方桂珍, 等. 湿热处理对玉米淀粉颗粒结构及热焓特性的影响[J]. 食品与发酵工业,2004,30(10):17−20. [ZHAO K, ZHANG S W, FANG G Z, et al. Effects of HMT on the granule and crystalline property of maize starch[J]. Food and Fermentation Industries,2004,30(10):17−20.ZHAO K, ZHANG S W, FANG G Z, et al. Effects of HMT on the granule and crystalline property of maize starch[J]. Food and Fermentation Industries, 2004, 30(010): 17-20. -