• EI
  • Scopus
  • 食品科学与工程领域高质量科技期刊分级目录第一方阵T1
  • DOAJ
  • EBSCO
  • 北大核心期刊
  • 中国核心学术期刊RCCSE
  • JST China
  • FSTA
  • 中国精品科技期刊
  • 中国农业核心期刊
  • CA
  • WJCI
  • 中国科技核心期刊CSTPCD
  • 中国生物医学SinoMed
中国精品科技期刊2020
张红雨, 宋曙辉, 周家华, 刘建福, 周连第. 紫山药低醇发酵饮料中乙醇含量的气相色谱法测定[J]. 食品工业科技, 2014, (01): 307-309. DOI: 10.13386/j.issn1002-0306.2014.01.023
引用本文: 张红雨, 宋曙辉, 周家华, 刘建福, 周连第. 紫山药低醇发酵饮料中乙醇含量的气相色谱法测定[J]. 食品工业科技, 2014, (01): 307-309. DOI: 10.13386/j.issn1002-0306.2014.01.023
ZHANG Hong-yu, SONG Shu-hui, ZHOU Jia-hua, LIU Jian-fu, ZHOU Lian-di. Determination of alcohol in purple yam low-alcohol fermented beverage by gas chromatography[J]. Science and Technology of Food Industry, 2014, (01): 307-309. DOI: 10.13386/j.issn1002-0306.2014.01.023
Citation: ZHANG Hong-yu, SONG Shu-hui, ZHOU Jia-hua, LIU Jian-fu, ZHOU Lian-di. Determination of alcohol in purple yam low-alcohol fermented beverage by gas chromatography[J]. Science and Technology of Food Industry, 2014, (01): 307-309. DOI: 10.13386/j.issn1002-0306.2014.01.023

紫山药低醇发酵饮料中乙醇含量的气相色谱法测定

Determination of alcohol in purple yam low-alcohol fermented beverage by gas chromatography

  • 摘要: 建立了紫山药低醇发酵饮料中乙醇含量的气相色谱检测方法。HP-INNOWAX(30m×0.25mm×25μm)毛细管柱为样品分析柱时,甲醇为样品的稀释剂;正丙醇可作为乙醇定量分析的内标物。甲醇、乙醇、正丙醇的出峰时间分别为2.909、3.110、3.846min,乙醇与正丙醇的分离度大于30。乙醇浓度在0.26.0mg/mL范围时,内标法测定的乙醇浓度与乙醇的峰面积的相关系数为0.9996,紫山药样品中乙醇的最低检出限为0.05mg/mL。该测定方法的乙醇回收率在94.4%107.4%之间,重复性实验的相对标准偏差(RSD)为4.23%,可满足紫山药低醇发酵饮料中乙醇含量的测定要求。 

     

    Abstract: A method for gas chromatography determinnation of alcohol content in purple yam low-alcohol femented beverages was reported in this paper. The samples were separated on HP- INNOWAX ( 30m × 0.25mm × 25μm) capillary column.Methanol was chosen as the diluent and the n- propanol was used as the standard substance. Results showed that the peak time of methanol, ethanol and n- propanol was 2.909, 3.110 and 3.846min, respectively.And the degree of separation for ethanol and n- propanol was more than 30. The linear range was 0.26.0mg /mL with a correlation of 0.9996, and the detection limits were 0.05mg /mL for alcohol in purple yam. Recoveries varied from 94.4% 107.4%, and the relative standard deviation ( RSD) of the repetitive experimental was 4.23%. This method developed could be used to detect alcohol content in purple yam low- aocohol femented beverages.

     

/

返回文章
返回