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中国精品科技期刊2020
张飞, 谷令彪, 秦召, 陈孟起, 霍现宽, 何保江, 秦广雍, 庞会利. 三种方法提取蒲公英净油中挥发性和半挥发性香味成分比较分析[J]. 食品工业科技, 2016, (20): 83-89. DOI: 10.13386/j.issn1002-0306.2016.20.008
引用本文: 张飞, 谷令彪, 秦召, 陈孟起, 霍现宽, 何保江, 秦广雍, 庞会利. 三种方法提取蒲公英净油中挥发性和半挥发性香味成分比较分析[J]. 食品工业科技, 2016, (20): 83-89. DOI: 10.13386/j.issn1002-0306.2016.20.008
ZHANG Fei, GU Ling-biao, QIN Zhao, CHEN Meng-qi, HUO Xian-kuan, HE Bao-jiang, QIN Guang-yong, PANG Hui-li. Comparative analysis of volatile and semi-volatile flavor components of Taraxacum mongolicum Hand.Mazz.absolute oils extracted by three methods[J]. Science and Technology of Food Industry, 2016, (20): 83-89. DOI: 10.13386/j.issn1002-0306.2016.20.008
Citation: ZHANG Fei, GU Ling-biao, QIN Zhao, CHEN Meng-qi, HUO Xian-kuan, HE Bao-jiang, QIN Guang-yong, PANG Hui-li. Comparative analysis of volatile and semi-volatile flavor components of Taraxacum mongolicum Hand.Mazz.absolute oils extracted by three methods[J]. Science and Technology of Food Industry, 2016, (20): 83-89. DOI: 10.13386/j.issn1002-0306.2016.20.008

三种方法提取蒲公英净油中挥发性和半挥发性香味成分比较分析

Comparative analysis of volatile and semi-volatile flavor components of Taraxacum mongolicum Hand.Mazz.absolute oils extracted by three methods

  • 摘要: 分别用亚临界流体、超临界CO2和有机溶剂萃取法提取蒲公英净油,对比不同提取方法所得蒲公英净油中挥发性和半挥发性香味成分的差异,使用GC-MS法进行定性分析,并采用峰面积归一法进行了半定量分析。三种方法提取所得净油中相对含量最高的均为十六酸,分别为66.881%(亚临界)、31.632%(超临界)和33.570%(乙酸乙酯);醛类物质含量最高的是亚临界净油,为6.218%;酮类和醇类物质含量最高的是超临界净油,为5.641%和4.072%;酯类物质含量最高的是乙酸乙酯净油,为21.202%。通过不同萃取方法之间的对比,为以后有针对性的提取蒲公英成分、进一步开发蒲公英资源提供数据支持。 

     

    Abstract: To compare volatile and semi- volatile flavor components of Taraxacum mongolicum Hand.Mazz.absolute oil extracted by three methods,subcritical fluid,supercritical CO_2 fluid and organic solvent,respectively.Moreover,qualitative and semi- quantitative analysis of all obtained absolute oil samples was determined by GC- MS method and peak area normalization method. To the relative content,hexadecanoic acid was the highest of all three extracted absolute oil,which were 66.881% in subcritical fluid extract,31.632% in supercritical CO_2 fluid extract,and33.570% in ethyl acetate extract,respectively.Of all,the highest content of aldehydes was subcritical fluid extract,which accounted for 6.218%,ketones and alcohols were highest in supercritical CO_2 fluid extract,for 5.641% and4.072%,ethyl acetate extract had the highest content of esters,for 21.202%. Through the comparison among different methods of extraction,this research aimed to provide data for the targeted extracts of Taraxacum mongolicum Hand.Mazz.components,and then supported further development of Taraxacum mongolicum Hand.Mazz.

     

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