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中国精品科技期刊2020
平洪睿,刘雯玄,杨金香,等. 山桐子油增香工艺的响应面法优化及其品质特性研究[J]. 食品工业科技,2025,46(23):229−241. doi: 10.13386/j.issn1002-0306.2024100178.
引用本文: 平洪睿,刘雯玄,杨金香,等. 山桐子油增香工艺的响应面法优化及其品质特性研究[J]. 食品工业科技,2025,46(23):229−241. doi: 10.13386/j.issn1002-0306.2024100178.
PING Hongrui, LIU Wenxuan, YANG Jinxiang, et al. Optimization of Idesia polycarpa Maxim Oil's Aroma-enhancing Process through Response Surface Methodology and Its Quality Traits Analysis[J]. Science and Technology of Food Industry, 2025, 46(23): 229−241. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2024100178.
Citation: PING Hongrui, LIU Wenxuan, YANG Jinxiang, et al. Optimization of Idesia polycarpa Maxim Oil's Aroma-enhancing Process through Response Surface Methodology and Its Quality Traits Analysis[J]. Science and Technology of Food Industry, 2025, 46(23): 229−241. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2024100178.

山桐子油增香工艺的响应面法优化及其品质特性研究

Optimization of Idesia polycarpa Maxim Oil's Aroma-enhancing Process through Response Surface Methodology and Its Quality Traits Analysis

  • 摘要: 本研究旨在以山桐子粕酶解液为主要原料,通过响应面法优化增香条件,得到山桐子增香油的最佳制备工艺。并以气相色谱-离子迁移谱技术(gas chromatography-ion mobility spectrometry,GC-IMS)、气相色谱法(gas chromatography,GC)和国标法对增香前后的山桐子油品质进行对比分析。结果表明:制备山桐子增香油的最佳工艺参数为:料油比(体积比)1:12、反应温度121 ℃、反应时间37 min。在此条件下山桐子油的增香效果最佳,综合感官评分达到9.16±0.58分。3-甲基丁醛、苯乙醛、2-乙酰基噻唑和2-甲基丙酸等物质赋予了山桐子增香油丰富的果香、脂香和肉香风味特征,对山桐子油的风味提升起到了关键作用。此外,山桐子增香油在烘烤香、焦糖香和综合感官评分方面均优于山桐子精炼油,在脂肪酸组成、酸价、过氧化值、色泽和皂化值等指标上与精炼油无显著性差异(P>0.05)。综上所述,山桐子油的增香技术有效地增强了山桐子精炼油的风味特征,同时保留了其原有品质特性,为山桐子油的产品开发和市场应用提供了科学依据。

     

    Abstract: This study aimed to optimize the aroma-enhancing conditions for Idesia polycarpa oil using response surface methodology, with enzyme-hydrolyzed I. polycarpa meal as the main raw material. The quality of the oil before and after aroma enhancement was analyzed by gas chromatography-ion mobility spectrometry (GC-IMS), gas chromatography (GC), and national standard methods. The results indicated that the optimal process parameters for preparing aroma-enhanced I. polycarpa oil were as follows: a material-to-oil ratio (v:v) of 1:12, a reaction temperature of 121 ℃, and a reaction time of 37 minutes. Under these conditions, the aroma-enhancing effect of I. polycarpa oil was optimal, with a comprehensive sensory score of 9.16±0.58. 3-Methylbutanal, phenylacetaldehyde, 2-acetylthiazole, and 2-methylpropionic acid endowed aroma-enhanced I. polycarpa oil with rich fruity, lipid, and meaty flavor characteristics, playing a crucial role in enhancing the flavor of I. polycarpa oil. Furthermore, in terms of baking aroma, caramel aroma, and comprehensive sensory evaluation, the aroma-enhanced I. polycarpa oil outperformed the refined I. polycarpa oil. When compared to the refinedoil, there was no significant difference in fatty acid composition, acid value, peroxide value, color, and saponification value (P>0.05). In conclusion, the aroma-enhancing technology of I. polycarpa oil effectively improved the flavor characteristics of refined I. polycarpa oil while maintaining its original quality features. This provided a scientific basis for the product development and market application of I. polycarpa oil.

     

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