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中国精品科技期刊2020
段京瑶,刘丽莉,邵贝贝,等. 微波真空冷冻干燥对基于3D打印固型的银耳多糖-蛋清蛋白-玉米淀粉复合凝胶特性的影响J. 食品工业科技,2026,47(12):1−9. doi: 10.13386/j.issn1002-0306.2025050093.
引用本文: 段京瑶,刘丽莉,邵贝贝,等. 微波真空冷冻干燥对基于3D打印固型的银耳多糖-蛋清蛋白-玉米淀粉复合凝胶特性的影响J. 食品工业科技,2026,47(12):1−9. doi: 10.13386/j.issn1002-0306.2025050093.
DUAN Jingyao, LIU Lili, SHAO Beibei, et al. Effects of Microwave Vacuum Freeze-drying on the Properties of Tremella Polysaccharide-Egg White Protein-Corn Starch Composite Gel Based on 3D Printing SolidificationJ. Science and Technology of Food Industry, 2026, 47(12): 1−9. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2025050093.
Citation: DUAN Jingyao, LIU Lili, SHAO Beibei, et al. Effects of Microwave Vacuum Freeze-drying on the Properties of Tremella Polysaccharide-Egg White Protein-Corn Starch Composite Gel Based on 3D Printing SolidificationJ. Science and Technology of Food Industry, 2026, 47(12): 1−9. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2025050093.

微波真空冷冻干燥对基于3D打印固型的银耳多糖-蛋清蛋白-玉米淀粉复合凝胶特性的影响

Effects of Microwave Vacuum Freeze-drying on the Properties of Tremella Polysaccharide-Egg White Protein-Corn Starch Composite Gel Based on 3D Printing Solidification

  • 摘要: 本研究旨在探讨不同浓度(0、0.06、0.08、0.10、0.12、0.14、0.16 g/mL)的玉米淀粉(CS)对银耳多糖-蛋清蛋白(TFP-EWP)复合凝胶3D打印精确度的影响,以及不同微波真空冷冻干燥时间(0、20、40、60、80、100、120和140 min)对打印产品固型效果的影响。以TFP-EWP-CS凝胶为原料,对不同浓度CS打印产品的打印精确度进行表征,采用微波真空冷冻干燥技术对其进行干燥处理,并对打印产品的水分含量、干燥速率、几何形状、质构、色差及水分分布等进行系统性评估。结果表明,CS添加量为0.12 g/mL时,TFP-EWP-CS复合凝胶3D打印偏差最低,打印偏差值为0.75%,随着干燥时间的延长,自由水比例显著下降,同时部分弱结合水转化为自由水并随之蒸发,产品的水分含量和干燥速率均呈下降趋势。在20、40、60和80 min的处理时间内,打印产品的形状基本保持稳定,固型保真度均大于90%,但直径和高度显著减少(P<0.05)。当干燥时间达到100 min时,产品表面出现裂缝。随着干燥时间的增加,产品的硬度、胶黏性和咀嚼性均显著增强,微波真空冷冻干燥处理使得产品的白度增加而黄度降低(P<0.05)。综上所述,本研究为优化TFP-EWP-CS复合凝胶打印产品的干燥工艺提供了方案参考。

     

    Abstract: This study aimed to investigate the effects of different concentrations (0, 0.06, 0.08, 0.10, 0.12, 0.14, 0.16 g/mL) of corn starch (CS) on the 3D printing accuracy of tremella polysaccharide-egg white protein (TFP-EWP) composite gels, as well as the influence of varying microwave vacuum freeze-drying times (0, 20, 40, 60, 80, 100, 120 min and 140 min) on the solidification properties of the printed products. TFP-EWP-CS gels with different CS concentrations were used as the raw material, and the printing accuracy of the products was characterized. Microwave vacuum freeze-drying was applied as the drying method, and the products were systematically evaluated for moisture content, drying rate, geometric shape, texture, color difference, and moisture distribution. The results indicated that at a CS concentration of 0.12 g/mL, the 3D printing deviation of the TFP-EWP-CS composite gel was the lowest, with a deviation value of 0.75%. As the drying time increased, the proportion of free water significantly decreased, while some weakly bound water converted to free water and subsequently evaporated, leading to a decline in both moisture content and drying rate. During the processing times of 20, 40, 60, and 80 min, the shape of the printed products remained relatively stable, with a solidification fidelity greater than 90%; however, both the diameter and height significantly decreased (P<0.05). Surface cracking was observed at 100 min of drying. As drying time increased, the hardness, adhesiveness, and chewiness of the products significantly enhanced, while the microwave vacuum freeze-drying treatment increased the whiteness and reduced the yellowness of the products (P<0.05). In conclusion, this study provides valuable references for optimizing the drying process of TFP-EWP-CS composite gel printing products.

     

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