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中国精品科技期刊2020
袁翔宇,徐敏,张瑾莉,等. 基于卵白蛋白与低聚果糖为壁材的香榧籽油微胶囊制备及其稳定性分析J. 食品工业科技,2026,47(18):1−10. doi: 10.13386/j.issn1002-0306.2025070018.
引用本文: 袁翔宇,徐敏,张瑾莉,等. 基于卵白蛋白与低聚果糖为壁材的香榧籽油微胶囊制备及其稳定性分析J. 食品工业科技,2026,47(18):1−10. doi: 10.13386/j.issn1002-0306.2025070018.
YUAN Xiangyu, XU Min, ZHANG Jinli, et al. Preparation and Stability Analysis of Torreya grandis Seed Oil Microcapsules Using Ovalbumin and Fructooligosaccharide as Wall MaterialsJ. Science and Technology of Food Industry, 2026, 47(18): 1−10. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2025070018.
Citation: YUAN Xiangyu, XU Min, ZHANG Jinli, et al. Preparation and Stability Analysis of Torreya grandis Seed Oil Microcapsules Using Ovalbumin and Fructooligosaccharide as Wall MaterialsJ. Science and Technology of Food Industry, 2026, 47(18): 1−10. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2025070018.

基于卵白蛋白与低聚果糖为壁材的香榧籽油微胶囊制备及其稳定性分析

Preparation and Stability Analysis of Torreya grandis Seed Oil Microcapsules Using Ovalbumin and Fructooligosaccharide as Wall Materials

  • 摘要: 为拓宽香榧籽油在食品工业中的功能化应用,本实验以卵白蛋白(ovalbumin,OVA)和低聚果糖(fructooligosaccharide,FOS)为复合壁材,经喷雾干燥,制备香榧籽油微胶囊。通过粒径、ζ-电位、微观形态及贮藏稳定性对乳液进行表征,分析微胶囊粉末的理化性质、微观形貌、氧化稳定性、热稳定性及体外模拟消化特性,研究不同比例FOS-OVA复合壁材组合得到的微胶囊性能。结果显示,以OVA-FOS为壁材、香榧籽油为芯材能形成稳定的水包油型乳液,其中,2%(w/w)OVA和18%(w/w)FOS的壁材比例能实现20%(w/w)香榧籽油负载量的微胶囊制备。所形成的微胶囊结构致密,对香榧籽油的包埋率达71.96%,兼具良好的溶解度(61.78%)、流动性(休止角36.83°)与贮藏性(水分含量3.72%)。加速氧化实验证实,微胶囊能有效保护香榧籽油,过氧化值和硫代巴比妥酸值较未包埋油脂分别降低了53.30%和66.06%,氧化稳定性显著提升。热重分析表明,微胶囊在200 ℃以下具有良好的稳定性,能满足食品热加工需要。同时,微胶囊化香榧籽油在体外模拟消化过程中具有较好的缓释特性。本研究可为香榧籽油微胶囊产品的开发及功能性油脂的有效保护提供理论方法参考,同时为开发功能性油脂食品提供新思路。

     

    Abstract: To broaden the functional applications of Torreya grandis seed oil in the food industry, mixtures of ovalbumin (OVA) and fructooligosaccharides (FOS) in varying proportions were employed as wall materials to prepare microcapsules of Torreya grandis seed oil via spray drying. The emulsions were characterized in terms of particle size, ζ-potential, micromorphology, and storage stability. The physicochemical properties, micromorphology, oxidative stability, thermal stability, and in vitro simulated digestion behavior of the microcapsule powders were also analyzed. The results indicated that stable oil-in-water (O/W) emulsions could be formed using OVA-FOS as wall materials with Torreya grandis seed oil as the core. Notably, a wall material ratio of 2 % (w/w) OVA and 18 % (w/w) FOS enabled the successful encapsulation of 20 % (w/w) Torreya grandis seed oil. Encapsulation efficiency of 71.96 % was achieved with a dense structure of Torreya grandis seed oil microcapsules, along with excellent solubility (61.78%), flowability (angle of repose 36.83°) and storage stability (moisture content 3.72%). Accelerated oxidation tests confirmed that the microcapsules effectively protected Torreya grandis seed oil. The peroxide value and thiobarbituric acid value were reduced by 53.30% and 66.06% respectively, compared with the unencapsulated oil, indicating a significant improvement in oxidative stability. Thermogravimetric analysis demonstrated that the microcapsules exhibited excellent stability below 200 ℃, meeting the thermal processing requirements for food applications. Furthermore, the microencapsulated Torreya grandis seed oil showed superior slow-release characteristics during simulated in vitro digestion. This study provides a theoretical reference for the development of microencapsulated Torreya grandis seed oil products and the effective protection of functional oils, offering new perspectives for the development of functional oil-based foods.

     

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