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中国精品科技期刊2020
奥斯曼·努尔艾合麦提,冯作山,尼格尔热依·亚迪卡尔,等. 基于HS-SPME-GC-MS 分析不同品种馕挥发性风味特征及关键成分J. 食品工业科技,2026,47(16):1−13. doi: 10.13386/j.issn1002-0306.2025070214.
引用本文: 奥斯曼·努尔艾合麦提,冯作山,尼格尔热依·亚迪卡尔,等. 基于HS-SPME-GC-MS 分析不同品种馕挥发性风味特征及关键成分J. 食品工业科技,2026,47(16):1−13. doi: 10.13386/j.issn1002-0306.2025070214.
OSMAN Nurahmat, FENG Zuoshan, NIGARY Yadikar, et al. Based on HS-SPME-GC-MS Analysis of Volatile Flavor Characteristics and Key Components in Multiple Varieties of NaanJ. Science and Technology of Food Industry, 2026, 47(16): 1−13. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2025070214.
Citation: OSMAN Nurahmat, FENG Zuoshan, NIGARY Yadikar, et al. Based on HS-SPME-GC-MS Analysis of Volatile Flavor Characteristics and Key Components in Multiple Varieties of NaanJ. Science and Technology of Food Industry, 2026, 47(16): 1−13. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2025070214.

基于HS-SPME-GC-MS 分析不同品种馕挥发性风味特征及关键成分

Based on HS-SPME-GC-MS Analysis of Volatile Flavor Characteristics and Key Components in Multiple Varieties of Naan

  • 摘要: 为推动新疆馕产业升级中的风味标准化控制,本文选取芝麻馕、洋葱馕及窝窝馕三种新疆特色馕为研究对象,利用顶空固相微萃取-气相色谱-质谱联用(Head Space Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry,HS-SPME-GC-MS)技术,系统分析了采用电加热馕坑烤制的三种馕的挥发性成分组成与差异。结果表明:三种馕样品共鉴定出110种挥发性化合物,包括醇类5种、醛类22种、酮类19种、羧酸类4种、酯类6种、醚类4种、烃类28种、吡嗪类14种及其他类8种。其中,芝麻馕、洋葱馕与窝窝馕分别检出66、87与56种挥发性成分,三者共有成分为42种。通过相对气味活性值(Relative Odor Activity Value,ROAV)与正交偏最小二乘判别分析(Orthogonal Projections to Latent Structures Discriminant Analysis,OPLS-DA),筛选出22种对整体风味具有重要贡献的关键风味物质(ROAV >1),并确定了21种用于区分不同馕品的大于等于1的差异标志物(Variable Importance in Projection,VIP)。三类馕的主体香气特征差异显著,具体表现为洋葱馕的含硫化合物贡献突出,芝麻馕以不饱和醛类与吡嗪类协同呈香,而窝窝馕则以吡嗪类主导其烘烤风味。本研究证实,原料配方的不同是导致馕品风味差异的主要原因,研究结果为新疆馕的风味定向调控与标准化工业生产提供了重要的数据支撑与理论依据。

     

    Abstract: To support the flavor standardization in the industrial upgrading of Xinjiang naan, this study investigated three characteristic varieties-sesame naan, onion naan, and wowo naan. The volatile aroma profiles of electric-baked naan were systematically analyzed using headspace solid-phase microextraction coupled with gas chromatography–mass spectrometry (HS-SPME-GC-MS). A total of 110 volatile compounds were identified across the samples, categorized into 5 alcohols, 22 aldehydes, 19 ketones, 4 carboxylic acids, 6 esters, 4 ethers, 28 hydrocarbons, 14 pyrazines, and 8 other compounds. Specifically, 66, 87, and 56 volatile components were detected in sesame naan, onion naan, and wowo naan, respectively, with 42 compounds common to all three. By applying relative odor activity value (ROAV) and orthogonal projections to latent structures discriminant analysis (OPLS-DA), 22 key aroma compounds (ROAV>1) and 21 discriminant markers (VIP≥1) were identified. Significant differences were observed in the dominant aroma characteristics: Sulfur-containing compounds imparted a distinct note to onion naan, unsaturated aldehydes and pyrazines synergistically contributed to the aroma of sesame naan, while pyrazines were the primary contributors to the roasted flavor of wowo naan. These findings demonstrate that ingredient composition is the main factor driving flavor differences, which providing a scientific basis for the targeted flavor regulation and standardized production of Xinjiang naan.

     

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